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Front Cover -- Integrated Analytical Approaches for Pesticide Management -- Copyright Page -- Contents -- List of Contributors -- Disclaimer -- 1 Introduction -- References -- 1 Setting the Framework -- 2 Generic Guidelines on Integrated Analytical Approaches to Assess Indicators of Pesticide Management Practices at a Catchm... -- Introduction -- Overall Strategy: "Black-Box" Monitoring -- Role of Laboratory in Fostering GAP -- Definition of Stakeholders, Roles, and Responsibilities -- Definition and Elaboration of the Strategy for Monitoring GAP -- Formation of the Working Team -- Selecting and Characterizing the Microcatchment -- Elaborate the Strategy -- Undertake a First-Tier Risk Assessment -- Initial Monitoring Strategy: The "Black-Box" Approach -- Where?-Selection of the Geo-Referencing Sampling Sites -- When?-Sampling Times and Frequencies -- What?-Matrices Sampled -- How Much?-Amounts Sampled -- How to Sample?-Sampling Tools and Procedures -- Who?-The Sampling Team -- Minimum Infrastructure and Tools -- Integrated Monitoring -- Data Interpretation and Assessment of Indicators of Pesticide Management Practice -- Interpretation of Monitoring Data -- Assessment of Indicators -- Outreach and Outcomes -- Laboratory Outreach -- Lesson Identified -- Outcomes -- References -- 2 Sampling -- 3 Sampling Strategies -- Introduction to Sampling and Monitoring -- Sampling for Decision Making -- What Types of Decisions Will Be Made? -- Defining Decision Rules -- Sampling Designs -- Simple Random Sampling -- Stratified Sampling -- Systematic Sampling -- Special Case 1: Transect Sampling -- Special Case 2: Grid Sampling -- Cluster Sampling -- Concepts of Accuracy, Bias, and Precision -- Spatial and Temporal Variation -- Spatial Considerations -- Temporal Considerations -- Field Sampling -- Soil -- Streams -- Spray Drift -- Use of Composite Sampling.

Front Cover -- Analytical Methods for Agricultural Contaminants -- Copyright Page -- Dedication -- Disclaimer -- Contents -- List of Contributors -- Glossary of terms -- 1 Introduction to the Book of Methods -- 2 General Requirements for Food Safety Analysis -- Setting Up a Residues Laboratory -- Define the mandate of the laboratory -- Establish the scope -- Define the types of methods and limitations desired -- Determine the analytical equipment requirements to perform the laboratory's tasks -- Define requirements for sustainability of the laboratory -- Specify the conditions of the analytical laboratory -- Examples of resources -- Sampling in the Context of Food Safety -- Sample Preparation and Processing -- Quality Assurance and Quality Control Procedures -- Method Validation -- Uncertainty Estimation -- Choosing the Right Method for Your Purpose -- References -- Further Reading -- 3 Integrated Analytical Approaches for Food Safety and Environmental Sustainability -- Examples of Methods for Food Contaminant Analysis -- METHOD 1: Pesticide residue determination in fresh fruits and vegetables using ethyl acetate extraction and QuEChERS clean-up -- METHOD 2: Extraction of pesticide residues present in fresh fruits and vegetables using the QuECHERS method -- METHOD 3: Analysis of pesticide residues by HPLC MS/MS in fresh fruits and vegetables -- METHOD 4: Pesticide residue determination in potato using the dispersive QuEChERS template with ammonium acetate -- METHOD 5: Multiresidue method for pesticides in potato using by QuECHERS and GC-MSD detection -- METHOD 6: Processing and extraction of fruits and vegetables with possible pesticide residue content -- METHOD 7: Determination of selected pesticides in tomato samples by column extraction and gel permeation chromatography cle